(2) Operation operation: When using a jacket device, the pressure to slowly heat up. To advance through the 0.1MP pressure, holding a quarter of an hour, and then slowly introduced into the vapor pressure of the operation, enamel reactor company, if conditions permit, according to the actual situation of the unit, to identify suitable heating and cooling curve, general control 3 ℃ / min or less. Equipment operation, should pay attention to the flange, then set the seal case manholes and packing boxes, such as find a leak should take immediate measures; autoclave after use, need to be unload operation. Uninstall process for the autoclave is very important, concrete steps are as follows: 1, cleaning, enamel reactor, must be cleaned kettle lid, sampling valve, while under water in the kettle case, enamel reactor Which is good, a little bit of nitrogen charge. 2, temporarily unused reactor, enamel reactor, preferably added to the reactor volume of 70% ethanol soaked clean, you can not tighten the screws. 3, the reaction solvent from the vent filled the kettle, after most of the residue washed. Injecting water half kettle stirred for 10 minutes at which time the kettle before opening the lid, the inner wall of the tank for cleaning.